Mironova Labs

TMHD Precursors for Optical Coatings

High-purity halide-free oxide deposition for AR and filter coatings

For optical coating engineers depositing ZrO₂ and rare-earth oxide films by ALD/CVD

≥99%

Assay Purity

28+

TMHD Metal Complexes

Halide-Free

No F/Cl Contamination

US-Made

Domestic Supply

Supported by peer-reviewed research≥99% purityHalide-freeUS-manufacturedSublimation-grade

Photonic integrated circuits and metamaterial coatings require conformal, high-purity oxide films on complex 3D geometries. Mironova’s halide-free TMHD precursors enable ALD deposition of rare-earth oxides (Er₂O₃, Gd₂O₃, Y₂O₃) with sub-nanometer thickness control and no halide-induced absorption losses.

Challenges & Solutions

Your Challenge. Our Answer.

We understand the specific problems you face — and we built solutions for each one.

The Problem

Halide contamination from chloride precursors creates absorption sites that degrade optical performance in AR and filter coatings

Mironova’s Answer

TMHD precursors are entirely halide-free — no Cl or F contamination. Stoichiometric, high-transparency oxide films.

The Problem

Precursor instability in heated delivery lines leads to particle generation and coating defects

Mironova’s Answer

TMHD ligands provide exceptional thermal stability during transport, minimizing particulate contamination

Published Research

Published Evidence

Key findings from peer-reviewed literature relevant to your application.

High-Purity ZrO₂ Films

Zr(TMHD)₄/O₃ ALD produces stoichiometric ZrO₂ with <0.5 at.% C and H impurities — suitable for optical-grade coatings.

Putkonen et al., J. Mater. Chem. 2001

Halide-Free Advantage

Halide precursors leave 1–3 at.% residual Cl that creates absorption sites in optical films. TMHD eliminates this pathway.

Park et al., J. Phys. Chem. C 2016

Market Context

Photonic Integration Demands Conformal Oxide Films

Photonic integrated circuits (PICs) and metamaterial optical coatings require conformal, high-quality oxide films on complex 3D geometries where traditional sputtering and sol-gel methods struggle. ALD-deposited rare-earth oxides (Er₂O₃, Gd₂O₃, Y₂O₃) enable waveguide amplifiers, optical signal processing, and quantum communication applications. Photonic integration is a rapidly growing market as data center and telecom infrastructure shifts toward photonics-based solutions.

Yole; LightCounting; Mironova analysis

High

PIC materials growth rate

ALD

Conformal deposition advantage

Application Notes

Optical Coating ALD Parameters

Zr(TMHD)₄/O₃: 375–400 °C, GPC 0.24 Å/cycle.
Gd(TMHD)₃/O₃: 250–300 °C, GPC ~0.3 Å/cycle.
Sublimation-grade purity minimizes optical scattering.
Ozone (O₃) required as oxidant.
For full ALD windows, vapor pressure curves, and peer-reviewed studies, please visit our Metal-Organic Precursors Science Hub.

Why Mironova

Your Advantage with Mironova

01

Rare-Earth Oxide Expertise

Er(TMHD)₃, Gd(TMHD)₃, and Y-based TMHD complexes for ALD-deposited optical waveguides, gain media, and high-refractive-index coatings.

02

Conformal 3D Coverage

ALD provides uniform film thickness on complex photonic geometries — trenches, pillars, and curved surfaces where line-of-sight methods fail.

03

Halide-Free Deposition

TMHD precursors eliminate Cl and F contamination that can increase optical absorption losses in waveguide and coating applications.

04

Custom Precursor Design

Need a specific metal-TMHD complex not in our catalog? We synthesize custom precursors with analytical characterization matched to your process requirements.

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FAQ

Frequently Asked Questions

Common technical questions about this product line, answered by our scientific team.

ALD provides sub-nanometer thickness control and truly conformal coverage on 3D photonic structures. For applications requiring uniform oxide films on complex geometries (waveguides, MEMS, photonic crystals), ALD is often the only viable deposition method.
Published results include Er₂O₃ waveguide amplifiers achieving 14.4 dB net gain at 1.54 µm, and Gd₂O₃ films with refractive index ~1.75–1.95. Al₂O₃/Y₂O₃ nanolaminates have achieved ~1.6 dB/cm propagation loss.
Yes. The TMHD platform supports diverse metal oxides with controllable refractive indices for metamaterial and multi-layer optical coating designs. Contact us to discuss your specific material stack requirements.

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Receive precursor samples with full analytical data for optical coating process development.

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Related Resources

Technical data, product specifications, and application guidance.