Mironova Labs

DMTMM for Aqueous Bioconjugation

Outperforms EDC/NHS in water — no persistent residues, no pre-activation

For bioconjugation and ADC scientists working with carboxyl-amine coupling in aqueous buffers

Supported by peer-reviewed research≥99% purity (HPLC)Water-soluble reagent & byproductsUS-manufacturedPublished comparisons vs EDC/NHS

Your Challenge. Our Answer.

We understand the specific problems you face — and we built solutions for each one.

The Problem

EDC/NHS requires tight pH control (optimal 3.5–4.5) and pre-activation timing — a reproducibility nightmare at scale

Mironova’s Answer

DMTMM·Cl activates carboxylic acids directly in water at pH 6–8 by simple mixing. No pre-activation step, no pH shifts required.

The Problem

EDC conjugation yields are often <20% for polysaccharide-protein vaccine conjugates at manufacturing scale

Mironova’s Answer

DMTMM produced higher degrees of substitution than EDC/NHS across all tested substrate classes in systematic comparisons

The Problem

EDC/NHS leaves persistent N-acylurea residues on surfaces that cannot be removed even after repeated washing

Mironova’s Answer

DMTMM produces water-soluble byproducts (2-hydroxy-4,6-dimethoxy-triazine) — clean surfaces, simple dialysis cleanup

Published Evidence

Key findings from peer-reviewed literature relevant to your application.

Superior Substitution vs EDC/NHS

DMTMM yielded superior degrees of substitution vs EDC/NHS across all tested substrates at matched feed ratios, without requiring pH control.

D’Este et al., Carbohydrate Polymers 2014

Persistent EDC Residues

EDC/NHS left persistent N-acylurea byproducts on CNF surfaces that could not be removed even after repeated washing and dialysis. DMTMM avoided this.

Kumar et al., Communications Chemistry 2023

Low EDC Conjugation Yields

In EDC-based vaccine conjugate manufacturing, "considerably less than 20% of the activated PS becomes conjugated."

Frasch, Vaccine 2009

Aqueous Bioconjugation Protocol

  • Solvent: Water, phosphate buffer, or MES buffer (pH 6–8)
  • Equivalents: 1.0–5.0 eq relative to carboxyl groups
  • Temperature: RT to 37 °C
  • Time: 1–24 h (substrate-dependent)
  • No pre-activation step — add DMTMM·Cl directly to reaction mixture

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Related Resources

Technical data, product specifications, and application guidance.